NOVEL INSIGHTS INTO PHASE FORMATION AND ELECTRICAL RESISTIVITY OF FeSe ALLOY PREPARED BY POWDER METALLURGY METHOD

Authors

DOI:

https://doi.org/10.36547/ams.30.2.2033

Keywords:

FeSe, powder metallurgy, tetragonal, lattice, resistivity

Abstract

This study prepared the FeSe alloy using a powder metallurgy route. The Fe and Se powders were weighed at an atomic ratio of Fe:Se = 1.025:1 and milled for 5 hours. A simultaneous thermal analysis (STA) was performed to observe the behavior of the milled powder during thermal changes. After packing the milled powder in a stainless-steel tube, it was compacted. Investigation was performed to observe how the tetragonal FeSe phase forms at sintering temperatures of 718 K, 818 K, and 918 K. At a sintering temperature of 718 K, the tetragonal FeSe phase was formed, as determined by our quantitative analysis of XRD. The highest tetragonal FeSe phase fraction of 68.46 wt.% was obtained at a temperature of 918 K. The lattice constants of the tetragonal FeSe for the best sample were a = 0.3773 nm and c = 0.5520 nm. The resistivity test demonstrated that all samples have a conductor phenomenon exceeding 16 K, with a maximum Tc-onset value of 15.11 K.

Author Biographies

Sigit Dwi Yudanto, National Research and Innovation Agency

Senior Researcher - Research Center for Metallurgy

National Research and Innovation Agency - Republic of Indonesia

Dea Nita Deslia Sari, Universitas Sumatera Utara

Department of Physics

Ryan Fitriandhani, Institut Teknologi PLN

Department of Mechanical Engineering

Agung Imaduddin, National Research and Innovation Agency

Research Center for Advanced Materials

Andika Widya Pramono, National Research and Innovation Agency

Research Center for Advanced Materials

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Published

2024-06-18

How to Cite

Dwi Yudanto, S., Nita Deslia Sari, D., Fitriandhani, R., Imaduddin, A., & Widya Pramono, A. (2024). NOVEL INSIGHTS INTO PHASE FORMATION AND ELECTRICAL RESISTIVITY OF FeSe ALLOY PREPARED BY POWDER METALLURGY METHOD. Acta Metallurgica Slovaca, 30(2), 72–76. https://doi.org/10.36547/ams.30.2.2033

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